血液中酒精化合物的分析
| Instrument: | GC-2010 Plus AF + HS-20 |
|---|---|
| Headspace: | Oven Temp.: 85 °C Vial Warming Time: 15 min Vial Pressurization Time: 1 min Injection Time: 0.5 min Sample Line Temp: 150 °C Vial Volume: 20 mL Vial Agitation: Off Vial Pressurization: 100 kPa Load Time: 0.5 min Needle Flash Time: 0.5 min Transfer Line Temp: 150 °C |
| Column: | SH-Rtx™-BAC Plus 2, 30 m, 0.32 mm ID, 0.60 μm (P/N: 227-36263-01) SH-Rtx™-BAC Plus 1, 30 m, 0.32 mm ID, 1.80 μm (P/N: 227-36260-01) |
| Column Temp: | 40 °C |
| Inj.: | Split (split ratio: 20:1) |
| Carrier Gas: | He, 100 kPa |
| Detector: | FID, 250 °C |
| Makeup Gas: | He, 30 mL/min |
| Hydrogen: | 40 mL/min |
| Air: | 400 mL/min |
