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SH-Rxi™-PAH

Product overview
- Mid-polarity proprietary phase
- Ideal for EFSA PAH4 analysis—separates all priority compounds: benz[a]anthracene, chrysene, benzo[b]fluoranthene and benzo[a]pyrene.
- Best resolution of chrysene from interfering PAHs, triphenylene, and cyclopenta[cd]pyrene.
- Complete separation of benzo [b], [k], [j], and [a] fluoranthenes.

 

Application

PAHs (US EPA Method 8100)

Peaks
1. Naphthalene 10. Pyrene 19. Dibenz(a,h)acridine
2. 2-Methylnaphthalene 11. Benz[a]anthracene 20. Dibenz[a,j]acridine
3. 1-Methylnaphthalene 12. Chrysene 21. Indeno[1,2,3-cd]pyrene
4. Acenaphthylene 13. Triphenylene 22. Dibenz[a,h]anthracene
5. Acenaphthene 14. Benzo[b]fluoranthene 23. Benzo[ghi]perylene
6. Fluorene 15. Benzo[k]fluoranthene 24. 7H-Dibenzo[c,g]carbazole
7. Phenanthrene 16. Benzo(j)fluoranthene 25. Dibenzo[a,e]pyrene
8. Anthracene 17. Benzo[a]pyrene 26. Dibenzo(a,i)pyrene
9. Fluoranthene 18. 3-Methylcholanthrene 27. Dibenzo(a,h)pyrene
 
Column:   SH-Rxi™-17Sil MS, 30 m, 0.25 mm ID, 0.25 μm (P/N: 221-75916-30
Inj. Vol.:   0.5 μL splitless (hold 1.75 min)
Inj. Temp:   320 °C
Purge Flow:   75 mL/min
Oven Temp:   65 °C (hold 0.5 min) to 220 °C at 15 °C/min to 330 °C at 4 °C/min (hold 15 min)
Carrier Gas:   He, constant flow rate 2.0 mL/min
Detector:   FID, 320 °C